Analysis data for probe TP-030-1 and control TP-030n
TP-030-1
| 1H NMR (300nMHz, CDCl3) | δ 2.70 (1H, dt, J = 15.5, 4.7 Hz), 3.10 (1H, ddd, J = 15.6, 10.7, 4.7 Hz), 3.38 (3H, s), 3.54 (1H, td, J = 11.2, 4.3 Hz), 4.22 (1H, dt, J = 11.9, 5.0 Hz), 4.42 (1H, dd, J = 9.8, 8.3 Hz), 4.62 (1H, dd, J = 11.7, 10.2 Hz), 5.34 (2H, s), 5.96 (1H, dd, J = 11.7, 8.3 Hz), 7.11−7.26 (7H, m), 7.29−7.39 (3H, m) |
| 13C NMR (75 MHz, CDCl3) | δ 20.6, 35.6, 45.8, 51.2, 56.8, 74.8, 121.3, 122.6, 123.3, 125.7, 125.9, 127.2, 128.0, 128.3, 128.9, 135.8, 136.8, 142.7, 150.0, 161.4, 169.6 |
TP-030n
| 1H NMR (300nMHz, CDCl3) | δ 1.80−2.01 (4H, m), 2.24−2.42 (1H, m), 2.75 (1H, dt, J = 15.6, 4.8 Hz), 2.85−3.19 (5H, m), 3.38 (3H, s), 3.50−3.62 (1H, m), 4.05 (2H, d, J = 7.4 Hz), 4.24 (1H, dt, J = 12.0, 5.2 Hz), 4.43 (1H, dd, J = 9.9, 8.2 Hz), 4.64 (1H, dd, J = 11.5, 10.0 Hz), 5.93 (1H, dd, J = 11.7, 8.3 Hz), 7.10−7.34 (5H, m). |